The redox behavior of lead nitrate was studied voltammetrically in presence and absence of acetyl acetone using both platinum and new made glassy carbon electrodes in 0.1 M KCl supporting electrode. Composition of the oxidation and reduction processes well done also with new graphene electrode from the three discussed electrodes, glassy carbon electrode gave better separated waves for both reduction and oxidation processes. All mechanisms were discussed. Comparison with other electrodes also done in literature like carbon paste electrode and hand drawn pencil electrode, our new prepared glassy carbon electrode gave better results.
[1]
K.C. Honeychurch, J.P. Hart, D.C. Cowell, D.W.M. Arrigan, Sensors and Actuators, B 77(2001)642-652.
[2]
Z. Ezerskis and Z. Jusys, Journal of Applied Electrochemistry, 31 (2001) 1117-1124.
[3]
Sanaa Majid, Mamia El Rhazi, Aziz Amine, Antonella Curulli and Giuseppe Palleschi, Mikrochimica. Acta, 143(2003) 195-204.
[4]
Ngono Therese Rosie Lauriance, Rachida Najih and Abdelilah Chtaini, Pharmaceutica Analytica Acta, 5, 4 (2014)295.
[5]
Gaber A. M. Mersal and M. M. Ibrahim, Int. J. of Electrochim. Sci., 8(2013)5944-5960.
[6]
E.A. Gomaa, A.H. El-Askalany and M.N.H. Moussa, Rev. Roum. Chim., 32 (1987) 243.
[7]
M.A. Ghandour, R.A. Abo-Doma and E.A. Gomaa. Electrochim. Acta, 27(1982) 159.
[8]
Esam A. Gomaa, Research and Reviews: Journal of Chemistry 3(2014) 28-37.
[9]
Esam A. Gomaa, A. H. El-Askalany and M, N, H, Moussa, Rev Roum. Chim, 3(1987) 243.
[10]
Esam A Gomaa, Theromochimica Acta, 128 (1988)99.
[11]
Esam A Gomaa, Indian J. of Tech., 24 (1986) 725 and E.A. Gomaa. Thermochim. Acta, 80 (1984) 355.
[12]
Esam A Gomaa, Croatica Chimica Acta, 62 (1989)475.
[13]
E.A. Gomaa, A.M. Shallapy and M.N.H. Moussa. Asian J. of Chem., 4, 518 (1992).
[14]
A.K. Abd-Elkader, E.A. Gomaa and A.H. El-Askalany, Acta Chimica Hung., 118(1985)197.
[15]
E.A. Gomaa, Y.A. Elewady and A.H. El-Askalany, Rev. Roum. de. Chimie, 35(1990)491.
[16]
A.M. El-Wakil, E.A. Gomaa and A.H. El-Askalany, Asian J.of Chem., 4(1992)523.
[17]
Esam A Gomaa, Thermochimica Acta, 91(1985)235 and A.B. Kashyout, H. M. A. Soliman, Marwa Fathy, E.A Gomaa and Ali Zidan, International Journal of photoenergy, (2012) 1-7.
[18]
Esam A Gomaa, Theromchimica Acta, 128(1988) 287 and Esam A. Gomaa, Frontiers in Science, 2(2012)24-27.
[19]
Esam A Gomaa, Thermochimica Acta, 140(1989) 7 and E. A. Gomaa, K.M. Ibrahim and N.M. Hassan, The international Journal of Engineering and Science (IJES), 3(2014)44-51.
[20]
Esam A Gomaa, Bull, Soc. Chim, Fr., 5(1989)620 and E.A. Gomaa, H.M. Abu El-Nader, Sh. E. Rashed, Physical Chemistry, 2012,2(3); 9-17.
[21]
Esam A Gomaa, Bull. Soc. Chim Fr., 5(1989) 371.
[22]
Esam A Gomaa, Thermochimica Acta, 152 (1989) 371 and T. Lanez, A. Rebiai, M. A. Saha, M. Alia, International Journal of Toxicology and Applied Pharmacology, 1(20, (2012)21-24.
[23]
Esam A Gomaa, Thermochimica Acta, 156 (1989) 91 and Kevin C. Honeychurch, Analytical Methods, 7(2015)2437-2443.
[24]
I. S. Shehatta, A. H. El-Askalany and E. A. Gomaa, Thermochimica Acta, 219(1993).
[25]
E. A. Gomaa, M.A. Mousa and A.A. El-Khouly. Thermochim. Acta, 86 (1985) 351.
[26]
Esam A. Gomaa and R. M. Galal, Basic Sciences of Medicine, 1(2) (2012): 1-5.
[27]
E.A. Gomaa, A.M. Shallaby and M. N. H. Moussa, J. Indian Chem. Soc., 68 (1991) 339.
[28]
M. A. Hamada E. A. Gamaa and N. A. Elshishtawi, International Journal of Optoelectronic Engineering, 1(2012)1-3.
[29]
E. A. Gomaa, M. A. Mostafa and F. I. El-Dossouki. Syn., React. Inorg. Mat. Org. Chem., 30(1), 157 (2000).
[30]
Esam A Gomaa, and B. A. M. Al-Jahdali, American Journal of Environmental Engineering, 2(2012) 6-12.
[31]
Nagah A. Shishtawi, Maany A. Hamada and Esam A. Gomaa, J. Chem. Eng. Data, 2010, 55 (12) pp.5422-5424.
[32]
Esam A. Gomaa and Mohamed A. Tahoon, Journal of Molecular Liquids 214(2016) 19-23.
